Search results for "Polymethacrylic Acids"

showing 10 items of 29 documents

Nanoparticles of a polyaspartamide-based brush copolymer for modified release of sorafenib: In vitro and in vivo evaluation.

2017

Abstract In this paper, we describe the preparation of polymeric nanoparticles (NPs) loaded with sorafenib for the treatment of hepatocellular carcinoma (HCC). A synthetic brush copolymer, named PHEA-BIB-ButMA (PBB), was synthesized by Atom Trasnfer Radical Polymerization (ATRP) starting from the α-poly( N -2-hydroxyethyl)- d , l -aspartamide (PHEA) and poly butyl methacrylate (ButMA). Empty and sorafenib loaded PBB NPs were, then, produced by using a dialysis method and showed spherical morphology, colloidal size, negative ζ potential and the ability to allow a sustained sorafenib release in physiological environment. Sorafenib loaded PBB NPs were tested in vitro on HCC cells in order to e…

3003MaleHepatocellular carcinomamedicine.medical_treatmentPharmaceutical Science02 engineering and technologyATRPPharmacology01 natural sciencesDrug Delivery SystemsCopolymerChemistryATRP; Hepatocellular carcinoma; Sorafenib; Tumor targeting; α-Poly(N-2-hydroxyethyl)-DL-aspartamide; 3003Liver NeoplasmsSorafenib021001 nanoscience & nanotechnologyDrug delivery0210 nano-technologymedicine.drugSorafenibNiacinamideCarcinoma HepatocellularCell SurvivalRadical polymerizationIntraperitoneal injectionL-aspartamideMice NudeAntineoplastic AgentsEnhanced permeability and retention effect010402 general chemistryPolymethacrylic AcidsIn vivoCell Line TumormedicineAnimalsHumansneoplasmsProtein Kinase InhibitorsPhenylurea Compoundstechnology industry and agriculturedigestive system diseasesIn vitro0104 chemical sciencesDrug LiberationTumor targetingDelayed-Action PreparationsBiophysicsα-Poly(N-2-hydroxyethyl)-DNanoparticlesα-Poly(N-2-hydroxyethyl)-DL-aspartamidePeptidesJournal of controlled release : official journal of the Controlled Release Society
researchProduct

PHEA-graft-polymethacrylate supramolecular aggregates for protein oral delivery

2013

Abstract Salmon calcitonin (sCT) is characterized by a poor oral availability. A new copolymer, β-poly(N-2-hydroxyethyl)-graft-{N-2-ethylene[2-poly(methacrylic acid sodium salt)isobutyrate]}- d , l -aspartamide (PHEA-IB-p(MANa + )), was designed for the oral administration of sCT through the formation of supramolecular aggregates (SAs) based on electrostatic interactions. Several sCT/PHEA-IB-p(MANa + ) weight ratios were characterized by turbidimetry, DLS, zeta potential, and microscopy analysis. After the incubation of sCT/PHEA-IB-p(MANa + ) complex with digestive enzymes, 10% (w/w) of loaded sCT was released in the native form. In vitro investigation was carried out to determine the copol…

Calcitoninmedicine.medical_specialtypeptide deliveryAdministration OralPharmaceutical Sciencechemistry.chemical_elementPeptidePharmacologyCalciumRats Sprague-DawleyRandom AllocationDrug Delivery SystemsPolymethacrylic AcidsPharmacokineticsimmune system diseasesOral administrationhemic and lymphatic diseasesmedicineAnimalsHumansPolyhydroxyethyl Methacrylatechemistry.chemical_classificationDrug CarriersGeneral Medicineoral deliveryRatsBioavailabilitySurgeryoral delivery; peptide delivery; calcitoninsurgical procedures operativechemistryCalcitoninSettore CHIM/09 - Farmaceutico Tecnologico ApplicativoPharmacodynamicsFemaleTurbidimetryCaco-2 CellsPeptidestherapeuticshuman activitiesPHEA oral delivery osteoporosis supramolecolar aggregates peptide almon calcitoninBiotechnology
researchProduct

Erzeugung von Sarkomen durch Fremdkörper aus Polymethacrylaten und Zusätzen

1962

Es wird uber die cancerogene Wirkung von Plattchen aus verschiedenen Kunststoffen berichtet (s. Tabelle).

Cancer ResearchOncologyChemistryPolymethacrylic AcidsGeneral MedicineMolecular biologyForeign BodiesZeitschrift für Krebsforschung
researchProduct

Effect of cyclic loading on fracture strength and microleakage of a quartz fiber dowel with different adhesive, cement and resin core material combin…

2010

Background: This study evaluated the performance of different adhesive-cement-core combinations coupled with quartz fiber dowels after cyclic loading and fracture strength tests and assessed the microleakage using dye penetration method. Methods: Forty maxillary canines (n=10 per group) were restored with fiber dowels (Quartz fiber DT Light Post) and four adhesive-cement-core material combinations [(Group 1: All-Bond 2+C&B (root) / All-Bond 2+Biscore (core); Group 2: All-Bond 2+Bisfil 2B (root) / All-Bond 2+Bisfil 2B (core); Group 3: Scotchbond 1+RelyX ARC (root) / Scotchbond 1+Supreme (core); Group 4: RelyX Unicem (root) / Scotchbond 1+Filtek Supreme (core)]. The specimens were initially c…

CuspidDental CementsEquipment DesignQuartzCyclic loading Fiber dowels Fracture strength MicroleakageComposite ResinsPermeabilityPolyethylene GlycolsResin CementsWeight-BearingResins SyntheticPolymethacrylic AcidsSettore MED/28 - Malattie OdontostomatologicheDentin-Bonding AgentsMaterials TestingMethacrylatesBisphenol A-Glycidyl MethacrylateEquipment FailureStress MechanicalPost and Core Technique
researchProduct

Polymeric microcontainers improve oral bioavailability of furosemide.

2016

Microcontainers with an inner diameter of 223 μm are fabricated using the polymer SU-8, and evaluated in vitro, in situ and in vivo for their application as an advanced oral drug delivery system for the poorly water soluble drug furosemide. An amorphous sodium salt of furosemide (ASSF) is filled into the microcontainers followed by applying a lid using Eudragit L100. It is possible to control the drug release in vitro, and in vitro absorption studies show that the microcontainers are not a hindrance for absorption of ASSF. In situ perfusion studies in rats are performed with ASSF-filled microcontainers coated with Eudragit and compared to a furosemide solution. The absorption rate constant …

Eudragit l100PolymersPharmaceutical ScienceAdministration OralBiological Availability02 engineering and technologyAbsorption (skin)PharmacologyMicro devices030226 pharmacology & pharmacy03 medical and health sciences0302 clinical medicineDrug Delivery SystemsPolymethacrylic AcidsIn vivoDelivery systemsFurosemideOral bioavailabilitymedicineAnimalsHumansIntestinal MucosaRats WistarIntestinal mucusChromatographyChemistryFurosemide021001 nanoscience & nanotechnologyBioavailabilityDrug LiberationMucusOral deliveryEpoxy CompoundsFemaleDelivery systemIntestinal perfusionCaco-2 Cells0210 nano-technologyOral retinoidmedicine.drugInternational journal of pharmaceutics
researchProduct

Histidine-rich glycoprotein-induced vascular normalization improves EPR-mediated drug targeting to and into tumors

2018

Tumors are characterized by leaky blood vessels, and by an abnormal and heterogeneous vascular network. These pathophysiological characteristics contribute to the enhanced permeability and retention (EPR) effect, which is one of the key rationales for developing tumor-targeted drug delivery systems. Vessel abnormality and heterogeneity, however, which typically result from excessive pro-angiogenic signaling, can also hinder efficient drug delivery to and into tumors. Using histidine-rich glycoprotein (HRG) knockout and wild type mice, and HRG-overexpressing and normal t241 fibrosarcoma cells, we evaluated the effect of genetically induced and macrophage-mediated vascular normalization on th…

Histidine-rich glycoproteinUT-Hybrid-DPharmaceutical ScienceVascular normalization02 engineering and technologyPermeabilityArticleMice03 medical and health scienceschemistry.chemical_compoundDrug Delivery Systems0302 clinical medicinePolymethacrylic AcidsCell Line TumorNeoplasmsmedicineAnimalsMethacrylamideTissue DistributionpHPMAFibrosarcomaMice Knockoutchemistry.chemical_classificationDrug CarriersProteins021001 nanoscience & nanotechnologymedicine.diseasePathophysiologyUp-RegulationMice Inbred C57BLHRGNanomedicineTumor targetingchemistryTargeted drug deliveryPermeability (electromagnetism)030220 oncology & carcinogenesisDrug deliveryDrug deliveryCancer researchEPR0210 nano-technologyGlycoprotein
researchProduct

Polymethacrylate monoliths with immobilized poly-3-mercaptopropyl methylsiloxane film for high-coverage surface functionalization by thiol-ene click …

2014

In this work, new polythiol-functionalized macroporous monolithic polymethacrylate-polysiloxane composite materials are presented which can be useful substrates for highly efficient immobilization of (chiral) catalysts, chromatographic ligands, and other functional moieties by thiol-ene click reaction. Poly(glycidyl methacrylate-co-ethylene dimethacrylate) (poly(GMA-co-EDMA)) monoliths were coated with a poly-3-mercaptopropyl methylsiloxane (PMPMS) film and subsequently the polymer was covalently immobilized by formation of crosslinks via nucleophilic substitution reaction with pendent 2,3-epoxypropyl groups on the monolith surface. This monolith, though, showed similar levels of surface co…

Hot TemperatureSiloxanesSurface PropertiesEpoxideBiochemistryAnalytical Chemistrychemistry.chemical_compoundPolymethacrylic AcidsCapillary ElectrochromatographyPolymer chemistryMethylmethacrylatesSulfhydryl CompoundsMonolithEne reactionAminationCapillary electrochromatographygeographygeography.geographical_feature_categoryChromatographyOrganic ChemistryEnantioselective synthesisReproducibility of ResultsGeneral MedicinechemistryClick chemistrySurface modificationChromatography LiquidJournal of Chromatography A
researchProduct

HPMA-LMA copolymer drug carriers in oncology: an in vivo PET study to assess the tumor line-specific polymer uptake and body distribution.

2013

Polymeric drug carriers aim to selectively target tumors in combination with protecting normal tissue. In this regard polymer structure and molecular weight are key factors considering organ distribution and tumor accumulation of the polymeric drug delivery system. Four different HPMA based copolymer structures (random as well as block copolymers with lauryl methacrylate as hydrophobic block) varying in molecular weight, size and resulting architecture were analyzed in two different tumor models (AT1 prostate carcinoma and Walker-256 mammary carcinoma) in vivo. Polymers were labeled with (18)F and organ/tumor uptake was followed by μPET imaging and ex vivo biodistribution. Vascular permeabi…

MaleBiodistributionPolymers and PlasticsBioengineeringVascular permeabilityBiomaterialschemistry.chemical_compoundPolymethacrylic AcidsIn vivoPolymer chemistryMaterials ChemistryDistribution (pharmacology)AnimalsTissue DistributionWhole Body ImagingCarcinoma 256 WalkerParticle SizeChemistryProstatic NeoplasmsIn vitroRatsDextranPositron-Emission TomographyBiophysicsMethacrylatesNanoparticlesRadiopharmaceuticalsDrug carrierEx vivoNeoplasm TransplantationBiomacromolecules
researchProduct

Freeze-dried eudragit-hyaluronan multicompartment liposomes to improve the intestinal bioavailability of curcumin.

2016

This work aimed at finding an innovative vesicle-type formulation able to improve the bioavailability of curcumin upon oral administration. To this purpose, phospholipid, Eudragit® S100 and hyaluronan sodium salt were combined to obtain eudragit-hyaluronan immobilized vesicles using an easy and environmentally-friendly method. For the first time, the two polymers were combined in a system intended for oral delivery, to enhance curcumin stability when facing the harsh environment of the gastrointestinal tract. Four different formulations were prepared, keeping constant the amount of the phospholipid and varying the eudragit-hyaluronan ratio. The freeze-drying of the samples, performed to inc…

MaleCurcuminPhospholipidPharmaceutical ScienceBiological Availability02 engineering and technology010402 general chemistry01 natural sciencesIntestinal absorptionchemistry.chemical_compoundFreeze-dryingPolymethacrylic AcidsAnimalsTissue DistributionHyaluronic AcidRats WistarLiposomeChromatographyVesicleGeneral Medicine021001 nanoscience & nanotechnology0104 chemical sciencesBioavailabilityRatsFreeze DryingchemistryIonic strengthLiposomesCurcumin0210 nano-technologyBiotechnologyEuropean journal of pharmaceutics and biopharmaceutics : official journal of Arbeitsgemeinschaft fur Pharmazeutische Verfahrenstechnik e.V
researchProduct

Improvement of the butyl methacrylate-paraffin embedment.

1983

The excellent butyl methacrylate-paraffin method as an embedment for light microscopy has been technically improved. More uniform and reproducible polymerization has been obtained by using a vacuum oven to degas the polymerizing mixture and to replace the air with nitrogen at 650 Torr. The amount of benzoyl peroxide required must be determined for each batch of butyl methacrylate. A teflon lined, reusable metal mold and a method of one-step blocking of tissues in preparation for sectioning are also described.

Materials scienceStaining and LabelingEmbedmentHistological Techniquestechnology industry and agriculturechemistry.chemical_elementBenzoyl peroxideNitrogenButyl methacrylateVacuum furnaceFixativeschemistryChemical engineeringPolymerizationPolymethacrylic AcidsParaffinTorrPolymer chemistryMicroscopymedicineMethacrylatesAnatomymedicine.drugStain technology
researchProduct